Friday, September 27, 2013

Gravimetric Determination of Phosphorus in Plant Food.

Abstract: gravimetric epitome provide be employ to sterilise the partage of phosphorus in coiffe food. A hurried of cognize root is p retinal roduced and weighed to go cover percent of phosphorus in compound. From the mass and known composition of the abrupt, the come in of original ion can be determined. Introduction: Gravimetric analysis is based on the step of mass. Gravimetric analysis involves isolation of an ion in solution by a hardihood reaction, filtering, washing the come down free of contaminants, vicissitude of the precipitate to a product of known composition, and finally measure the precipitate and find its mass by difference. From the mass and known composition of the precipitate, the amount of the original ion can be determined. Theodore W. Richards (1868-1928) and his polish students at Harvard developed or defined many of the techniques of gravimetric analysis of ash grey and chlorine. These techniques were used to determine the atomic w eights of 25 of the elements, decomposing known weights of the compounds, and find out the chloride content by gravimetric methods. Purpose: To find the percent of phosphorus in known compound MgNH4PO4*6H2O employ gravimetric analysis. Procedure: 1. Weigh by difference to the nearest hundreth one thousand .75 of your unknown sample, using weighing paper. Using solualbe Expert be food label percentate 30% P2O5. 2.
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Transfer the sample quantitatively to a 250-ml beaker and record the sample mass. 3. Add 18 ml of distilled water and stir the misture with a glass stirring rod to dissolve the sample. 4. To the filtrate add about 45ml of 10% MgSO4*7H2Osolution. 5. therefore add approxi mately 150ml of 2 M NH3(aq) while stirring. ! A white precipitate of MgNH4PO4*6H20will form. Allow the mixture to sit at room temperature for 15 minutes to complete the precipitation. 6. Collect the precipitate on a preweighed piece of filter paper. 7.Obtain a filter... If you commit to get a full essay, order it on our website: OrderEssay.net

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